HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → 3-methoxy-11-methyl-11H-s-triazolo[3,4-b][3] benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 21323329 | HCID 21323329 | — |
| Product | 3-methoxy-11-methyl-11H-s-triazolo[3,4-b][3] benzazepine | HCID 21323320 | — |
Reaction Steps
The reaction of 11-methyl-3-methylsulfonyl-11H-s-triazolo[3,4-b][3]benzazepine with sodium methoxide yielded 3-methoxy-11-methyl-11H-s-triazolo[3,4-b][3] benzazepine. Colorless prisms (as recrystallized from ether), melting point: 101°-102° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150139 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-c8593d6452b74e0ca7d2f74bd483df45 |
| Source note | uspto-grants-1979_04 |