反应详情

0.01 mol of 4-phenyl semicarbazide hydrochloride in solution in 10 ml water was added to a solution of 0.01 mol of 2-oximino indan-1,3-dione in 60 ml ethanol. The reaction mixture was refluxed for 1 hour. The precipitate formed was centrifuged when hot, dried and recrystallised from acetonitrile.

1. temperatureThe reaction mixture was refluxed for 1 hour
2. customThe precipitate formed
3. customdried
4. customrecrystallised from acetonitrile