Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Phenylsemicarbazide hydrochloride → 2-Oximino-1-(4-phenyl semicarbazono)-3-indanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Phenylsemicarbazide hydrochloride | HCID 79505 | — |
| 반응물 | 2-(Hydroxyimino)-1H-indene-1,3(2H)-dione | HCID 316190 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Oximino-1-(4-phenyl semicarbazono)-3-indanone | HCID 136381158 | — |
반응 단계
0.01 mol of 4-phenyl semicarbazide hydrochloride in solution in 10 ml water was added to a solution of 0.01 mol of 2-oximino indan-1,3-dione in 60 ml ethanol. The reaction mixture was refluxed for 1 hour. The precipitate formed was centrifuged when hot, dried and recrystallised from acetonitrile.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05648381 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-1778b1cf9298420f85defa4186ed0f03 |
| 출처 메모 | uspto-grants-1997_07 |