HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → HCID 4148530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | 4-(4 5-Diphenyl-2-imidazolyl)phenol* | HCID 352144 | — |
| Product | HCID 4148530 | HCID 4148530 | 63.1% |
Reaction Steps
2-(4-Hydroxyphenyl)-4,5-diphenylimidazole (5 g) (J. Org. Chem., 1964, 29, 1926) was reacted with 8-bromooctane (6.2 g) in a method similar to Example 9. Work-up and recrystallisation from ethanol and water gave 2-(4-octyloxyphenyl)-4,5-diphenylimidazole (4.29 g, 63%) as a white solid, m.p. 178°. Found: C, 82.31; H, 7.66; N, 6.73%; C29H32N2O requires C, 82.04; H, 7.60; N, 6.60%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648373 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-63253a76e5e74da2a9181d4035d43177 |
| Source note | uspto-grants-1997_07 |