HRID265387

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11430

Potassium Carbonate

CK2O3

HCID264813

Ethyl 8-bromooctanoate

C10H19BrO2

HCID54385773

4,5-Bis(4-bromophenyl)-1H-imidazole

C15H10Br2N2

PRODUCTS

生成物

结构：CCOC(=O)CCCCCCCn1cnc(-c2ccc(Br)cc2)c1-c1ccc(Br)cc1

HCID22916427

未命名化合物

收率 71.2%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

4,5-Di-(4-bromophenyl)imidazole (2.13 g) was treated with ethyl 8-bromooctanoate (2 g) and K2CO3 (0.5 g) in 2-butanone as described in Example 9 to give ethyl 8-(4,5-di-(4-bromophenyl)imidazol-1-yl)-octanoate (2.2 g, 52%) as a pale yellow oil.; Found: C, 55.13; H, 5.19; N, 5.18; Br; 28.76%; C28H28Br2N2O2 requires: C, 54.76; H, 5.15; N, 5.11; Br, 29.15%