4-Propyl-4-phenyl-4-silacyclohexanone → HCID 178418450, compound

Participants

Role	Name	HCID	Charge
Reactant	4-Propyl-4-phenyl-4-silacyclohexanone	HCID 11831317	—
Reactant	(4-Chloro-2,6-difluorophenyl)trimethylsilane	HCID 18935733	—
Reactant	4-Bromo-2,6-difluoro-1-(1,2-difluorovinyl)benzene	HCID 53800791	—
Product	HCID 178418450	HCID 178418450	—

Reaction Steps

The general procedure of Example 35 was repeated using 4-propyl-4-phenyl-4-silacyclohexanone instead of 4-pentyl-4-phenyl-4-silacyclohexanone, 4-chloro-2,6-difluorophenyltrimethylsilane instead of 4-chlorophenyltrimethylsilane, and 4-bromo-2,6-difluoro-1-(1,2-difluorovinyl)benzene instead of 4-bromo-2,6-difluoro-1-(2,2-difluorovinyloxy)benzene, thereby obtaining the intended compound.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US05730901
Source dataset	uspto-grants-1998_03
ORD ID	ord-cbb6a7ae64f8437f8e6e1b614d3b6cc8
Source note	uspto-grants-1998_03