HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → Octimibate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 8-Hydroxyoctanoic acid | HCID 69820 | — |
| Reactant | HCID 12675128 | HCID 12675128 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Octimibate | HCID 65676 | — |
Reaction Steps
1,4,5-Triphenyl-2-chloroimidazole was treated with 8-hydroxyoctanoic acid and sodium hydride in dimethylformamide to give the title compound, m.p. 158°-159° C., Found: C, 75.3; H, 6.6;N, 6.0%; C29H30N2O3.0.43H2O Requires: C, 75.3;H, 6.7; N, 6.0%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648373 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-76ac360b82104bbaa4280a81906f62fd |
| Source note | uspto-grants-1997_07 |