Hydrochloric Acid → HCID 14551713, compound

HRID 265645Notes

Reaction equation

HRID 265645 reaction equation
[Cl:1][C:2]1([C:10](=[O:12])[CH3:11])[CH2:7][CH:6]([CH2:8][CH3:9])OC1=O.[ClH:13]>>[Cl:1][CH:2]([CH2:7][CH:6]([Cl:13])[CH2:8][CH3:9])[C:10](=[O:12])[CH3:11]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 14551712HCID 14551712, compound

Product 1

HCID 14551713HCID 14551713, compound

Procedure

The title compound is prepared according to the method described in Example 1 starting from 49 g (0.26 moles) of α-chloro-α-acetyl-γ-ethyl-γ-butyrolactone and 98 cm3 of abs. hydrochloric acid. After distillation 22 g (47%) of the title compound is obtained. Its boiling point is 68°-70° C. at a pressure of 133.3 Pa, nD20 =1,4600.

Workup

  1. distillationAfter distillation 22 g (47%) of the title compound
  2. customis obtained

Sources & evidence

ORD record
ord-2f933b0caf834838a82f6f291b4d347f
Source dataset
uspto-grants-1997_07
Patent number
US05648498

Reaction notes

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