HRID265645

反应详情

EQUATION

反应方程式

HRID 265645 的结构方程式

PROCEDURE

实验过程

The title compound is prepared according to the method described in Example 1 starting from 49 g (0.26 moles) of α-chloro-α-acetyl-γ-ethyl-γ-butyrolactone and 98 cm3 of abs. hydrochloric acid. After distillation 22 g (47%) of the title compound is obtained. Its boiling point is 68°-70° C. at a pressure of 133.3 Pa, nD20 =1,4600.

WORKUP

后处理

  1. distillationAfter distillation 22 g (47%) of the title compound
  2. customis obtained