Triethylsilane → HCID 19034148, compound

Participants

Reaction Steps

A solution of 10-6 (0.225 g, 0.47 mmoles) in CH2Cl2 (5 ml) was treated with Et3SiH (0.33 g, 4.2 mmoles) at ambient temperature and the resulting solution was stirred for 18 hours. The solvent was removed and the residue was purified by flash chromatgraphy on silica gel eluting with EtOH(10)/H2O(1)/NH4OH(1) to give two components: 10-8 had Rf 0.25 under these conditions:

Provenance & Evidence