反应详情

A solution of 10-14 (0.05 g, 0.114 mmoles) in CH3OH (1 ml) was treated with 10% Pd/C (25 mg) and then hydrogenated for 2 hours at 1 atom H2. The catalyst was then removed by filtration. The solution concentrated to give pure 10-15. Rf 0.3 (silica, EtOH(10)/H2O(1)/NH4OH(1).

1. customThe catalyst was then removed by filtration
2. concentrationThe solution concentrated
3. customto give pure 10-15