HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86751083, compound → HCID 86751082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86751083 | HCID 86751083 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86751082 | HCID 86751082 | — |
Reaction Steps
A solution of 10-14 (0.05 g, 0.114 mmoles) in CH3OH (1 ml) was treated with 10% Pd/C (25 mg) and then hydrogenated for 2 hours at 1 atom H2. The catalyst was then removed by filtration. The solution concentrated to give pure 10-15. Rf 0.3 (silica, EtOH(10)/H2O(1)/NH4OH(1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648368 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-7650813296a140c3b6f1f32704a9653f |
| Source note | uspto-grants-1997_07 |