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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 265903Generated: November 1, 2026

Hydrochloric Acid → HCID 22874918, compound

https://huagongshe.com/reaction/265903

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 22874944HCID 22874944—
SolventEthyl AcetateHCID 8857—
ProductHCID 22874918HCID 22874918—

Reaction Conditions

Temperature0 °C

Reaction Steps

A solution of 28-4 (1.0 g, 1.8 mmol) in 10 mL EtOAc was cooled to -40° C. and saturated with HCl gas. The solution was warmed to 0° C., then concentrated to give 28-5 as a tan solid. Rf (10:1:1 EtOH/H2O/NH4OH) 0.18.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05648368
Source datasetuspto-grants-1997_07
ORD IDord-0ef3827d138f494988cde2585f6d80dc
Source noteuspto-grants-1997_07