HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 265903Generated: November 1, 2026
Hydrochloric Acid → HCID 22874918, compound
https://huagongshe.com/reaction/265903
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22874944 | HCID 22874944 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22874918 | HCID 22874918 | — |
Reaction Steps
A solution of 28-4 (1.0 g, 1.8 mmol) in 10 mL EtOAc was cooled to -40° C. and saturated with HCl gas. The solution was warmed to 0° C., then concentrated to give 28-5 as a tan solid. Rf (10:1:1 EtOH/H2O/NH4OH) 0.18.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05648368 |
|---|
| Source dataset | uspto-grants-1997_07 |
|---|
| ORD ID | ord-0ef3827d138f494988cde2585f6d80dc |
|---|
| Source note | uspto-grants-1997_07 |
|---|