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HRID266051

反应详情

EQUATION

反应方程式

HRID 266051 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Cc1cc(C)c(S(=O)(=O)[O-])c(C)c1.N[n+]1ccccc1
HCID13028200

未命名化合物

结构：CCCCC#CC(=O)c1ccc(Br)cc1
HCID54449136

未命名化合物

PRODUCTS

生成物

1
结构：CCCCc1nn2ccccc2c1C(=O)c1ccc(Br)cc1
HCID21472334

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

2 次

PROCEDURE

实验过程

A mixture of 2.5 g of N-aminopyridinium mesitylene sulfonate (prepared by Synthesis, 1977 page 1, TAMURA, et al.), 25 ml of acetonitrile and 3.5 g of potassium carbonate was stirred for 15 minutes at ambient temperature and then the 2.27 g of the product of Step A in solution in 25 ml of acetonitrile were added.