HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 70281469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 10624326 | HCID 10624326 | — |
| Product | HCID 70281469 | HCID 70281469 | — |
Reaction Steps
According to the same manner as that described in Example 14, ethyl 2-chloromethyl-4-(3-isopropoxy-4-methoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate was reacted with diethylamine to give ethyl 2-(N,N-diethylaminomethyl)-4-(3-isopropoxy-4-methoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate dihydrochloride. This compound was recrystallized from ethyl acetate - ether. Yellow powder, mp. 122°-124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05650410 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-f2489688aff94ad5a84aa810f05297bb |
| Source note | uspto-grants-1997_07 |