HRID266150

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID19032365

未命名化合物

结构：COc1ccc(C(=O)c2cc(OC)c(OC)cc2N)cc1OC.Cl

HCID21466134

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)c1c(CCCCN(CC)CC)nc2cc(OC)c(OC)cc2c1-c1ccc(OC)c(OC)c1

HCID19032373

未命名化合物

PROCEDURE

实验过程

According to the same manner as that described in Example 49, 2-amino-4,5,3',4'-tetramethoxybenzophenone hydrochloride was reacted with ethyl 7-(N,N-diethylamino)-3-oxoheptanoate to give ethyl 2-[4-(N,N-diethylamino)butyl]-4-(3,4-dimethoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate. This compound was recrystallized from ethyl acetate - hexane. Colorless prisms, mp. 171°-172° C.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-410955bb2e194b22bc233967dd45ed34
来源数据集: uspto-grants-1997_07
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05650410
来源说明: uspto-grants-1997_07

反应 SMILES

Cl.[NH2:2][C:3]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[CH:17][C:4]=1[C:5]([C:7]1[CH:12]=[CH:11][C:10]([O:13][CH3:14])=[C:9]([O:15][CH3:16])[CH:8]=1)=O.[CH2:25]([N:27]([CH2:30][CH2:31][CH2:32][CH2:33][C:34](=O)[CH2:35][C:36]([O:38][CH2:39][CH3:40])=[O:37])[CH2:28][CH3:29])[CH3:26]>>[CH2:25]([N:27]([CH2:30][CH2:31][CH2:32][CH2:33][C:34]1[C:35]([C:36]([O:38][CH2:39][CH3:40])=[O:37])=[C:5]([C:7]2[CH:12]=[CH:11][C:10]([O:13][CH3:14])=[C:9]([O:15][CH3:16])[CH:8]=2)[C:4]2[C:3](=[CH:20][C:19]([O:21][CH3:22])=[C:18]([O:23][CH3:24])[CH:17]=2)[N:2]=1)[CH2:28][CH3:29])[CH3:26]