HRID266153

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10988

1-Butanamine, 3-methyl-N-(3-methylbutyl)-

C10H23N

结构：CCOC(=O)c1c(CCl)nc2cc(OC)c(OC)cc2c1-c1ccc(OC)c(OC)c1

HCID10813243

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)c1c(CN(CCC(C)C)CCC(C)C)nc2cc(OC)c(OC)cc2c1-c1ccc(OC)c(OC)c1

HCID54145036

未命名化合物

PROCEDURE

实验过程

According to the same manner as that described in Example 33, ethyl 2-chloromethyl-4-(3,4-dimethoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate was reacted with diisopentylamine to give ethyl 4-(3,4-dimethoxyphenyl)-2-(N,N-diisopentylaminomethyl)-6,7-dimethoxyquinoline-3-carboxylate. This compound was recrystallized from ethyl acetate - hexane. Colorless prisms, mp. 114°-115° C.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-561a8a4e60fa4cc7ad69de828f18b7af
来源数据集: uspto-grants-1997_07
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05650410
来源说明: uspto-grants-1997_07

反应 SMILES

Cl[CH2:2][C:3]1[C:12]([C:13]([O:15][CH2:16][CH3:17])=[O:14])=[C:11]([C:18]2[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[C:20]([O:26][CH3:27])[CH:19]=2)[C:10]2[C:5](=[CH:6][C:7]([O:30][CH3:31])=[C:8]([O:28][CH3:29])[CH:9]=2)[N:4]=1.[CH2:32]([NH:37][CH2:38][CH2:39][CH:40]([CH3:42])[CH3:41])[CH2:33][CH:34]([CH3:36])[CH3:35]>>[CH3:27][O:26][C:20]1[CH:19]=[C:18]([C:11]2[C:10]3[C:5](=[CH:6][C:7]([O:30][CH3:31])=[C:8]([O:28][CH3:29])[CH:9]=3)[N:4]=[C:3]([CH2:2][N:37]([CH2:38][CH2:39][CH:40]([CH3:42])[CH3:41])[CH2:32][CH2:33][CH:34]([CH3:35])[CH3:36])[C:12]=2[C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH:23]=[CH:22][C:21]=1[O:24][CH3:25]