HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diisoamylamine → ethyl 4-(3,4-dimethoxyphenyl)-2-(N,N-diisopentylaminomethyl)-6,7-dimethoxyquinoline-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diisoamylamine | HCID 10988 | — |
| Edukt | Ethyl 2-chloromethyl-4-(3,4-dimethoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate | HCID 10813243 | — |
| Produkt | ethyl 4-(3,4-dimethoxyphenyl)-2-(N,N-diisopentylaminomethyl)-6,7-dimethoxyquinoline-3-carboxylate | HCID 54145036 | — |
Reaktionsschritte
According to the same manner as that described in Example 33, ethyl 2-chloromethyl-4-(3,4-dimethoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate was reacted with diisopentylamine to give ethyl 4-(3,4-dimethoxyphenyl)-2-(N,N-diisopentylaminomethyl)-6,7-dimethoxyquinoline-3-carboxylate. This compound was recrystallized from ethyl acetate - hexane. Colorless prisms, mp. 114°-115° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05650410 |
| Quelldatensatz | uspto-grants-1997_07 |
| ORD ID | ord-561a8a4e60fa4cc7ad69de828f18b7af |
| Quellennotiz | uspto-grants-1997_07 |