反应详情

To a solution of 53g (0.23 mol) 8-chloro-2-(n-propyl)amino-1,2,3,4-tetrahydronaphthalene and 50 ml triethylamine in 500 ml dichloromethane was added dropwise 33 ml (40 g, 0.28 mol) benzoylchloride. After stirring over night at room temperature, 10% sodium carbonate was added and the mixture was shaken and separated. The organic phase was dried (magnesium sulphate), filtered and evaporated yielding 72 g (95%) raw product.

1. stirringthe mixture was shaken
2. customseparated
3. dry with materialThe organic phase was dried (magnesium sulphate)
4. filtrationfiltered
5. customevaporated