HRID26628

反应详情

EQUATION

反应方程式

HRID 26628 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1 mole of 1-methylimidazole was dissolved in 400 ml of ethanol and 1.2 moles of n-octyl bromide were added. The mixture was then heated to the boiling point for 5 hours. Thereafter, ethanol and excess n-octyl bromide were removed. The residue was purified in ether. In this manner, 250 g of 1-n-octyl-3-methyl-imidazolium bromide were obtained.

WORKUP

后处理

  1. temperatureThe mixture was then heated to the boiling point for 5 hours
  2. customThereafter, ethanol and excess n-octyl bromide were removed
  3. customThe residue was purified in ether