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HRID266407

反应详情

EQUATION

反应方程式

HRID 266407 的结构方程式

REACTANTS

反应物

2
结构：C1CNCCN1
HCID4837

Piperazine

C4H10N2

结构：CC(=O)N[C@@H](CSSC[C@H](NC(C)=O)C(=O)O)C(=O)O
HCID6995101

未命名化合物

PRODUCTS

生成物

1
结构：C1C[NH2+]CCN1.CC(=O)N[C@@H](CSSC[C@H](NC(C)=O)C(=O)[O-])C(=O)[O-]
HCID131718840

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

To N,N'-diacetyl-L-cystine (4.60 mmole, 1.49 g) dissolved in 5 mL of water was added piperazine (4.60 mmole, 0.90 g). To the solution was added enough isopropanole to cause formation of an oil, which slowly solidifies. The salt was isolated and dried.

WORKUP

后处理

  1. additionTo the solution was added enough isopropanole
  2. customThe salt was isolated
  3. customdried