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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 266452Generated: October 30, 2026

m-Chloroperbenzoic acid → HCID 15392139, compound

https://huagongshe.com/reaction/266452

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
ReactantHCID 21758505HCID 21758505—
ProductHCID 15392139HCID 15392139—

Reaction Steps

Following a procedure similar to that described in Example 32A, 0.75 g (0.0023 mol) of 2-(2-pyrimidinylsulfinylmethyl)saccharin was oxidized with 0.4 g (0.0023 mol) of 3-chloroperbenzoic acid in 50 ml of MDC and the product recrystallized from 75:25 acetonitrile:ethanol to give 2-(2-pyrimidinylsulfonylmethyl)saccharin, mp 225°-227° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05650422
Source datasetuspto-grants-1997_07
ORD IDord-5bd77b62f119411f840ea58553bdc4c3
Source noteuspto-grants-1997_07