Hydrochloric Acid → 2-[Butyl(methyl)amino]ethan-1-ol--hydrogen chloride (1/1)

HRID 266669Notes

Reaction equation

HRID 266669 reaction equation
[ClH:1].[CH3:2][N:3]([CH2:8][CH2:9][OH:10])[CH2:4][CH2:5][CH2:6][CH3:7]>C(OCC)C>[ClH:1].[CH3:2][N:3]([CH2:8][CH2:9][OH:10])[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 2370412-(N-METHYL-N-BUTYLAMINO)ETHANOL

Product 1

HCID 190304022-[Butyl(methyl)amino]ethan-1-ol--hydrogen chloride (1/1)

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Hydrochloric acid (gas) was bubbled through a solution of 10.0 g (0.0762 mmol) of 2-(N-methyl-N-butylamino)ethanol in diethyl ether. The resultant solution was concentrated in vacuo to provide a gold oil.

Workup

  1. concentrationThe resultant solution was concentrated in vacuo
  2. customto provide a gold oil

Sources & evidence

ORD record
ord-e81260f2187b416f97980818ba9de356
Source dataset
uspto-grants-1997_07
Patent number
US05652213

Reaction notes

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