HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 657774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Ethyl 2-oxocyclopentanecarboxylate | HCID 69136 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 657774 | HCID 657774 | — |
Reaction Steps
100 mmol of 2-aminoaniline and 135 mmol of 2-ethoxycarbonylcyclopentanone in 50 ml of xylene are brought to reflux for 5 hours, the water and the ethanol formed being removed with the aid of a Dean and Stark apparatus. After cooling, the expected product crystallizes and it is then filtered, washed with xylene and then with hexane and then dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05652246 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-7ac6d9fe98f1498ba392bc96ea506c11 |
| Source note | uspto-grants-1997_07 |