HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54257986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Acetic acid, 2-(triphenylphosphoranylidene)-, methyl ester | HCID 17453 | — |
| Reactant | HCID 19030840 | HCID 19030840 | — |
| Product | HCID 54257986 | HCID 54257986 | — |
Reaction Steps
To N-(1-benzyl-4-piperidinyl)-2-formyl-3-methylaniline (7.0 g) are added methanol (100 ml) and methyl (triphenylphosphoranylidene)acetate (15 g) and the mixture is refluxed for 1 hour. After cooling, the formed crystals are separated by filtration to give methyl 2-methyl-5-[(1-benzyl-4-piperidinyl)amino]cinnamate (5.6 g) as pale yellow powders, m.p. 140°-142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05652247 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-854cc6c9580d4c9983d5e98e42023c7f |
| Source note | uspto-grants-1997_07 |