HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22875130, compound → HCID 22875156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22875130 | HCID 22875130 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22875156 | HCID 22875156 | 100.7% |
Reaction Steps
To a solution of 0.330 g of the intermediate obtained from Step A in 5 mL of ethanol at was added 1 drop of triethylamine and hydrogenated with hydrogen balloon for 3 h. The catalyst was filtered off through a pad of celite and washed with ethyl acetate. The filtrate was concentrated to give 0.269 g of the product as a colorless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05652235 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-40cd043345554fa9960a8ab3b3e4a0ad |
| Source note | uspto-grants-1997_07 |