Hydrochloric Acid → HCID 178499561, compound

HRID 267074Notes

Reaction equation

HRID 267074 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

Into a solution of 1H-imidazole-4-acetic acid hydrochloride (4 g, 24.6 mmol) in methanol (100 ml) was bubbled hydrogen chloride gas until saturated. This solution was allowed to stand for 18 h at room temperature and the solvent evaporated in vacuo to give (1) as a white solid.

Workup

  1. customthe solvent evaporated in vacuo

Sources & evidence

ORD record
ord-9a2dac9480ee48e7923f448ab3b67277
Source dataset
uspto-grants-1997_07
Patent number
US05652257

Reaction notes

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