Hydrochloric Acid → HCID 21555573, compound

HRID 267201Notes

Reaction equation

HRID 267201 reaction equation
[NH2:1][C:2]1[NH:7][CH:6]([C:8]2[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=2)[C:5]2=[C:16]([CH3:22])[N:17]=[C:18]([CH2:19][CH2:20][CH3:21])[N:4]2[N:3]=1.Cl>>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=2)[C:5]2=[C:16]([CH3:22])[N:17]=[C:18]([CH2:19][CH2:20][CH3:21])[N:4]2[N:3]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178440033HCID 178440033, compound

Product 1

HCID 21555573HCID 21555573, compound

Procedure

2-Amino-4(p-methoxyphenyl)-5-methyl-7-propylimidazo[5,1-f]-as-triazine was prepared from 2-amino-3,4-dihydro-4(p-methoxyphenyl)-5-methyl-7-propylimidazo[5,1-f]-as-triazine (Example 14b). It was converted to its hydrochloride, which was crystallised from a mixture of ethanol and ether and had m.p. 224°-226° (21%).

Workup

  1. customwas crystallised from a mixture of ethanol and ether

Sources & evidence

ORD record
ord-61ff2ac9b26d49789768fa31a72c267f
Source dataset
uspto-grants-1976_03
Patent number
US03941785

Reaction notes

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