Hydrochloric Acid → HCID 178440036, compound

HRID 267210Notes

Reaction equation

HRID 267210 reaction equation
[NH2:1][C:2]1[NH:7][CH:6]([CH:8]2[C:13](=[O:14])[NH:12][C:11](=[O:15])[NH:10][C:9]2=[O:16])[C:5]2=[C:17]([CH3:23])[N:18]=[C:19]([CH2:20][CH2:21][CH3:22])[N:4]2[N:3]=1.[ClH:24]>C(O)C.CCOCC>[ClH:24].[NH2:1][C:2]1[NH:7][CH:6]([CH:8]2[C:13](=[O:14])[NH:12][C:11](=[O:15])[NH:10][C:9]2=[O:16])[C:5]2=[C:17]([CH3:23])[N:18]=[C:19]([CH2:20][CH2:21][CH3:22])[N:4]2[N:3]=1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 178440035HCID 178440035, compound

Product 1

HCID 178440036HCID 178440036, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 3283Diethyl EtherSolvent

Procedure

5(2-Amino-3,4-dihydro-5-methyl-7-propylimidazo [5,1-f]-as-triazin-4-yl)barbituric acid (0.5 g.) in ethanol (10 ml.) was treated with a solution of hydrogen chloride in ether. The solid was collected and crystallised from a mixture of methanol and ether and had m.p. 200°-205°.

Workup

  1. customThe solid was collected
  2. customcrystallised from a mixture of methanol and ether

Sources & evidence

ORD record
ord-6866e9942b284958bedf46aa96d1585e
Source dataset
uspto-grants-1976_03
Patent number
US03941785

Reaction notes

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