Hydrazine hydrate (1:1) → HCID 86733096, compound

HRID 267272Notes

Reaction equation

HRID 267272 reaction equation
[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([Cl:12])[CH:7]=1)=O.O.[NH2:21][NH2:22]>C(O)COCCO>[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:3]=1[C:4](=[N:21][NH2:22])[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([Cl:12])[CH:7]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 5231026HCID 5231026, compound

Product 1

HCID 86733096HCID 86733096, compound

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In the manner given in Preparation 1, 2-amino-3'-chloro-5-nitrobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-3'-chloro-5-nitrobenzophenone hydrazone.

Sources & evidence

ORD record
ord-418ccb6dbbac4969bd2f4746eda72681
Source dataset
uspto-grants-1976_03
Patent number
US03941802

Reaction notes

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