Hydrazine hydrate (1:1) → 2-Amino-2'-chlorobenzophenone hydrazone

HRID 267402Notes

Reaction equation

HRID 267402 reaction equation
[NH2:1][C:2]1[CH:16]=[CH:15][CH:14]=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=O.O.[NH2:18][NH2:19]>C(O)COCCO>[NH2:1][C:2]1[CH:16]=[CH:15][CH:14]=[CH:13][C:3]=1[C:4](=[N:18][NH2:19])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12]

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 761652-Amino-2'-chlorobenzophenone

Product 1

HCID 867330942-Amino-2'-chlorobenzophenone hydrazone

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In the manner given in Preparation 1, 2-amino-2'-chlorobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-2'-chlorobenzophenone hydrazone.

Sources & evidence

ORD record
ord-58c3ad7c057543cab63c0675e420a7d2
Source dataset
uspto-grants-1976_03
Patent number
US03941803

Reaction notes

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