2-Amino-5-nitrobenzophenone → 2-Amino-5-nitrobenzophenone hydrazone

HRID 267406Notes

Reaction equation

HRID 267406 reaction equation
[NH2:1][C:2]1[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)=O.O.[NH2:20][NH2:21]>C(O)COCCO>[NH2:1][C:2]1[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][C:3]=1[C:4](=[N:20][NH2:21])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 2

HCID 156812-Amino-5-nitrobenzophenoneHCID 24654Hydrazine hydrate (1:1)

Product 1

HCID 783883702-Amino-5-nitrobenzophenone hydrazone

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In the manner given in Preparation 1, 2-amino-5-nitrobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-5-nitrobenzophenone hydrazone.

Sources & evidence

ORD record
ord-4595e2e51dd744ae8a1d4443645a198e
Source dataset
uspto-grants-1976_03
Patent number
US03941803

Reaction notes

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