HRID267407

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID14797

Potassium hydroxide

HKO

HCID4067448

Methanone, (2-amino-5-chlorophenyl)(2-chlorophenyl)-, hydrazone

C13H11Cl2N3

PRODUCTS

生成物

HCID14357874

4-Chloro-2-[(2-chlorophenyl)methyl]aniline

C13H11Cl2N

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8117

Diethylene glycol

C4H10O3

PROCEDURE

实验过程

In the manner given in Preparation 11, 2-amino-2',5-dichlorobenzophenone hydrazone is refluxed with potassium hydroxide in diethylene glycol to give 2-(o-chlorobenzyl)-4-chloroaniline, boiling point 140°-148° (0.15 mm Hg), melting point 64°-65° C.