HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 4-Chloro-2-[(2-chlorophenyl)methyl]aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Methanone, (2-amino-5-chlorophenyl)(2-chlorophenyl)-, hydrazone | HCID 4067448 | — |
| Solvent | Diethylene Glycol | HCID 8117 | — |
| Product | 4-Chloro-2-[(2-chlorophenyl)methyl]aniline | HCID 14357874 | — |
Reaction Steps
In the manner given in Preparation 11, 2-amino-2',5-dichlorobenzophenone hydrazone is refluxed with potassium hydroxide in diethylene glycol to give 2-(o-chlorobenzyl)-4-chloroaniline, boiling point 140°-148° (0.15 mm Hg), melting point 64°-65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03941803 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-5a77f532b0214cbdb4955431fd18e9eb |
| Source note | uspto-grants-1976_03 |