Formaldehyde → HCID 21555826, compound

HRID 267428Notes

Reaction equation

HRID 267428 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:23])[C:9]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[CH:11][C:10]=1[N:18]1[CH:22]=[CH:21][N:20]=[CH:19]1.[CH2:24]=[O:25]>C1(C)C(C)=CC=CC=1>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:23])[C:9]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[CH:11][C:10]=1[N:18]1[CH:22]=[CH:21][N:20]=[C:19]1[CH2:24][OH:25]

Participants

4

Reactant 2

HCID 712FormaldehydeHCID 13186913HCID 13186913, compound

Product 1

HCID 21555826HCID 21555826, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner given in Example 1, 2'-chloro-5-nitro-2-(imidazol-1-yl)benzophenone is heated in a bomb with paraformaldehyde in xylene to 140° C. to give 2'-chloro-5-nitro-2-[2-(hydroxymethyl)imidazol-1-yl]-benzophenone.

Sources & evidence

ORD record
ord-ae5b987c551349919e9985d951b9a8d5
Source dataset
uspto-grants-1976_03
Patent number
US03941803

Reaction notes

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