HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 8-chloro-6-(o-chlorophenyl)-2-methyl-4H-imidazo[1,2-a][1,4]benzodiazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 2',5-Dichloro-2-[4-methyl-2-(phthalimidomethyl)imidazol-1-yl]benzophenone | HCID 21555825 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 8-chloro-6-(o-chlorophenyl)-2-methyl-4H-imidazo[1,2-a][1,4]benzodiazepine | HCID 12707131 | — |
Reaction Steps
In the manner given in Example 25, 2',5-dichloro-2-[4-methyl-2-(phthalimidomethyl)imidazol-1-yl]benzophenone in ethanol is heated with hydrazine to give 8-chloro-6-(o-chlorophenyl)-2-methyl-4H-imidazo[1,2-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03941803 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-11714be9494e42f58eb070fafb2c7283 |
| Source note | uspto-grants-1976_03 |