Acetyl bromide → HCID 21555053, compound

Participants

Reaction Steps

One and one-half grams of (1-bromo-2-hydroxypropyl)phosphonic acid prepared from the sodium salt obtained in Example 22 is heated with 5 ml. of acetyl bromide for one hour. The excess acetyl bromide is distilled off under reduced pressure and ice-cold water is added to the residue. The solution is stirred at room temperature and lyophilized to give (1bromo-2-acetoxypropyl)phosphonic acid.

Provenance & Evidence