HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus sulfide (P2S5) → HCID 21555051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | HCID 21555085 | HCID 21555085 | — |
| Product | HCID 21555051 | HCID 21555051 | — |
Reaction Steps
One and one-quarter grams of (2-bromo-1-acetoxypropyl)phosphonic dichloride is heated with 0.55 g. of finely pulverized P2S5 under nitrogen at 130°C. for three hours. The reaction mixture is fractionally distilled to give threo (2-bromo-1-acetoxypropyl)phosphonothioic dichloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03943153 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-446c3a56af5341569398c5774a24b7c0 |
| Source note | uspto-grants-1976_03 |