HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 178504101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 14364274 | HCID 14364274 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178504101 | HCID 178504101 | — |
Reaction Steps
To a solution of 2.3 parts of diethyl (methylthio)-thiocarbonylphosphonate in 50 parts of dry tetrahydrofuran was added 1.5 parts of sodium iodide. The solution was stirred for 18 hours at room temperature, then warmed on a steam bath for one-half hour. The desired orange ethyl sodium (methylthio)thiocarbonylphosphonate was then filtered, m.p. 288°d.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03943201 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-9f8bd435296d48969ae82dc4e6e0d957 |
| Source note | uspto-grants-1976_03 |