HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloropyrazine → 2-Chloro-3-phenoxypyrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloropyrazine | HCID 78575 | — |
| Reactant | Phenolate Sodium | HCID 4445035 | — |
| Product | 2-Chloro-3-phenoxypyrazine | HCID 20528961 | — |
Reaction Steps
A suspension of 0.1 mole of sodium phenoxide and 0.1 mole 2,3-dichloropyrazine is refluxed 10-20 hours. The cooled mixture is extracted with diethyl ether, washed with cold 2N sodium hydroxide solution, dried, and evaporated to give 2-chloro-3-phenoxypyrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946009 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-be942f0565a844a5afad22dc7374412a |
| Source note | uspto-grants-1976_03 |