HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl oxalacetate → HCID 68133663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl oxalacetate | HCID 66951 | — |
| Reactant | 3-Fluoro-p-anisaldehyde | HCID 67696 | — |
| Reactant | 2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- | HCID 643756 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68133663 | HCID 68133663 | — |
Reaction Steps
After heating a solution of 17 g of 3-fluoro-4-methoxybenzaldehyde, 20.9 g of oxalacetic acid diethyl ester and 14.3 g of β-aminocrotonic acid ethyl ester in 80 ccs of ethanol under reflux, the mixture is evaporated in vacuo and the reaction product is obtained as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946028 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-b40eae7f4504422f975f579b862ab314 |
| Source note | uspto-grants-1976_03 |