HRID268072

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10434

1,3-Cyclohexanedione

C6H8O2

HCID88505

6-Nitroveratraldehyde

C9H9NO5

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC2=C(C(=O)CCC2)C1c1cc(OC)c(OC)cc1[N+](=O)[O-]

HCID70635419

未命名化合物

收率 52%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Boiling a solution of 8.5 g of 6-nitroveratraldehyde, 4.0 g of cyclohexane-1,3-dione and 5.2 g of amidinoacetic acid ethyl ester in 150 ml of ethanol for 1 hour yields 2-amino-4-(2-nitro-4,5-dimethoxyphenyl)-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3-carboxylic acid ethyl ester of melting point 261°C (ethanol).

WORKUP

后处理

customfor 1 hour