Potassium Hydroxide → HCID 54087479, compound

Participants

Reaction Steps

A mixture of 97 g (0.45 mole) of 5-(p-nitrophenyl)-2-furonitrile, 34 g (0.49 mole) of hydroxylamine hydrochloride, 27 g (0.49 mole) of KOH and 1450 ml of absolute ethanol was refluxed for one hour, cooled and filtered. The solid was stirred in dilute HCl/H2O, and was filtered and air dried to yield 86 g (67%). An analytical sample was prepared by drying a sample in the vacuum pistol at room temperature, m.p. 230°.

Provenance & Evidence