Potassium Hydroxide → HCID 54019477, compound

Participants

Reaction Steps

A mixture of 30 g (0.11 mole) of 5-(p-benzyloxyphenyl)-2-furonitrile, 8.3 g (0.12 mole) of hydroxylamine hydrochloride, 8 g (0.12 mole) of KOH and 330 ml of absolute ethanol was refluxed for 11/2 hours, cooled in an ice bath and filtered. The solid obtained was recrystallized from 95% ethanol to yield 19 g (56%). An analytical sample was obtained by drying a sample in the vacuum pistol at the temperature of refluxing CHCl3, m.p. 145°-146°.

Provenance & Evidence