Methanol → HCID 21549795, compound

Participants

Reaction Steps

A mixture of 3.17 g. (0.01 mole) of cyanuric bromide, 1.78 g sodium bicarbonate and 18 ml. methanol was heated under refluxing conditions with stirring for 2 hours. The mixture was cooled and diluted with 50 ml. water. The product was isolated by filtration, washed with water and dried, giving 1.79 g. of white solid, m.p. 118°-120°C.; crystallized from 75 ml. cyclohexane, m.p. 120°-121°C.

Provenance & Evidence