Cyanuric chloride → HCID 54317184, compound

HRID 268157Notes

Reaction equation

HRID 268157 reaction equation
[N:1]1[C:8]([Cl:9])=[N:7][C:5](Cl)=[N:4][C:2]=1[Cl:3].[C:10]1(=[O:20])[NH:14][C:13](=[O:15])[C:12]2=[CH:16][CH:17]=[CH:18][CH:19]=[C:11]12.[K]>CC(C)=O>[Cl:9][C:8]1[N:1]=[C:2]([Cl:3])[N:4]=[C:5]([N:14]2[C:13](=[O:15])[C:12]3=[CH:16][CH:17]=[CH:18][CH:19]=[C:11]3[C:10]2=[O:20])[N:7]=1

Participants

4

Reactant 2

HCID 7954Cyanuric chlorideHCID 24194345Phthalimide potassium salt

Product 1

HCID 54317184HCID 54317184, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

18.5 Grams cyanuric chloride, 18.5 grams potassium phthalimide and 200 ml. acetone were combined and stirred at 0°-5°C. for 7 hours. The reaction mixture was then allowed to warm to room temperature and stirred an additional 15 hours. The white slurry was filtered, washed with cold acetone, reslurried in 250 ml. cold water, filtered, washed with water and dried. On recrystallization from benzene, there was obtained 17 grams of product, m.p. 175°-179°C.

Workup

  1. stirringstirred an additional 15 hours
  2. filtrationThe white slurry was filtered
  3. washwashed with cold acetone
  4. filtrationcold water, filtered
  5. washwashed with water
  6. customdried
  7. customOn recrystallization from benzene

Sources & evidence

ORD record
ord-14df47b6443e431386daa7ff757b67fc
Source dataset
uspto-grants-1976_03
Patent number
US03947374

Reaction notes

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