HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 54510280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | 2H-3,1-Benzoxazine-2,4(1H)-dione, 1-methyl-6-nitro- | HCID 78414 | — |
| Reactant | L-Proline | HCID 145742 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54510280 | HCID 54510280 | — |
Reaction Steps
This compound is obtained when 1,2,3,11a-tetrahydro- 10-methyl-7-nitro-11H-pyrrolo[2,1-c] [1,4]benzodiazepin-5,11- (10H]-dione (prepared from proline and 5-nitro-N-methylisatoic anhydride by the procedure of Example 1) is treated with 1 M borane in tetrahydrofuran by the procedure of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947408 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-19c4eaa42ae1422a8786f3ca8fca5a37 |
| Source note | uspto-grants-1976_03 |