HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 3-(methylthio)- → HCID 178503176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 3-(methylthio)- | HCID 15693 | — |
| Reactant | HCID 178428198 | HCID 178428198 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178503176 | HCID 178503176 | — |
Reaction Steps
A mixture of 21.7 g. (0.1 m.) of the compound of Example I, C., 13.9 g. (0.1 m.) of 3-methylmercaptoaniline and 250 ml. of dimethylformamide was refluxed overnight with stirring. It was chilled, filtered, washed with ether and air-dried to give 29 g. m.p. 310°-313°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947434 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-7a207709f5e542a1a6bcd62f146b7786 |
| Source note | uspto-grants-1976_03 |