HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzylamine → HCID 178490943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Reactant | HCID 178428198 | HCID 178428198 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178490943 | HCID 178490943 | — |
Reaction Steps
A stirred mixture of the compound of Example I, C. (22 g. 0.1 mole) and p-methoxy-benzylamine (14 g. 0.1 mole) in 200 ml. of dimethylformamide was refluxed for 6 hours. The reaction solution was stripped in vacuo to give 35 g. (98%) of pale yellow solid. Recrystallization from CH3OH/ether gave m.p. 250°-255°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947434 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-2937d86850b44752bffcc0c2cc930f2c |
| Source note | uspto-grants-1976_03 |