HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanone, (4-methoxyphenyl)(2-phenyl-3-benzofuranyl)- → (4-Hydroxyphenyl)(2-phenyl-1-benzofuran-3-yl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanone, (4-methoxyphenyl)(2-phenyl-3-benzofuranyl)- | HCID 6613416 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Product | (4-Hydroxyphenyl)(2-phenyl-1-benzofuran-3-yl)methanone | HCID 13264991 | — |
Reaction Steps
3-(4-Methoxybenzoyl)-2-phenylbenzofuran (16.4 g., 0.05 mol.) is combined with 50 g. of freshly distilled pyridine hydrochloride and the mixture is refluxed 1 hour. The hot mixture is poured with stirring onto an ice-dilute hydrochloric acid mixture and the precipitate is collected to give 3-(4-hydroxybenzoyl)-2-phenylbenzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947470 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-0ce6b454a8994fe0a6e9a8453c75f8a3 |
| Source note | uspto-grants-1976_03 |