HRID268347

反应详情

EQUATION

反应方程式

HRID 268347 的结构方程式

PROCEDURE

实验过程

3-(3,5-Dimethyl-4-methoxybenzoyl)-2-phenylbenzofuran (17.8 g., 0.05 mol.) is combined with 50 g. of freshly distilled pyridine hydrochloride and the mixture is refluxed 1 hour. The hot mixture is poured with stirring onto an ice-dilute hydrochloric acid mixture and the precipitate is collected to give 3-(3,5-dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran.

WORKUP

后处理

  1. additionThe hot mixture is poured
  2. customthe precipitate is collected